C₄₇H₄₃N₃O₈

Base Information

Chemical Name:C₄₇H₄₃N₃O₈
CAS No.:1330717-11-7
Molecular Formula:C₄₇H₄₃N₃O₈
Molecular Weight:777.874
Hs Code.:

C<sub>47</sub>H<sub>43</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₄₇H₄₃N₃O₈

Suppliers and Price of C₄₇H₄₃N₃O₈

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₇H₄₃N₃O₈

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₇H₄₃N₃O₈

There total 14 articles about C₄₇H₄₃N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₉H₅₃N₃O₁₀

: 1330717-11-7
C₄₇H₄₃N₃O₈

Guidance literature:: With lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; at 70 ℃; for 30h;
DOI:10.1016/j.tet.2011.06.046

Reference yield:

: C₄₁H₄₉N₃O₈Si

: 1330717-11-7
C₄₇H₄₃N₃O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrogen fluoride; water / acetonitrile / 1.5 h / 0 °C

2.1: hydrogenchloride; water / 1,2-dimethoxyethane / 6 h / 40 °C

3.1: toluene-4-sulfonic acid / methanol / 18 h / 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 25 h / 20 °C

5.1: tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C / Inert atmosphere

5.2: 1.67 h / -78 - -50 °C / Inert atmosphere

6.1: toluene / 7 h / 110 °C / Inert atmosphere

7.1: pyridine; dmap / 17 h / 20 °C

8.1: acetic acid / 1 h / 40 °C

9.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; acetone / 0.33 h / 20 °C

9.2: 0 °C

10.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 30 h / 70 °C

With pyridine; hydrogenchloride; dmap; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; hydrogen fluoride; water; tert.-butyl lithium; toluene-4-sulfonic acid; acetic acid; lithium tri-t-butoxyaluminum hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; water; dimethyl sulfoxide; acetone; toluene; acetonitrile; pentane;
DOI:10.1016/j.tet.2011.06.046

Reference yield:

: C₃₇H₃₇N₃O₇

: 1330717-11-7
C₄₇H₄₃N₃O₈

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride; water / 1,2-dimethoxyethane / 6 h / 40 °C

2.1: toluene-4-sulfonic acid / methanol / 18 h / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 25 h / 20 °C

4.1: tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C / Inert atmosphere

4.2: 1.67 h / -78 - -50 °C / Inert atmosphere

5.1: toluene / 7 h / 110 °C / Inert atmosphere

6.1: pyridine; dmap / 17 h / 20 °C

7.1: acetic acid / 1 h / 40 °C

8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; acetone / 0.33 h / 20 °C

8.2: 0 °C

9.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 30 h / 70 °C

With pyridine; hydrogenchloride; dmap; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; water; tert.-butyl lithium; toluene-4-sulfonic acid; acetic acid; lithium tri-t-butoxyaluminum hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; water; dimethyl sulfoxide; acetone; toluene; pentane;
DOI:10.1016/j.tet.2011.06.046