[closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

Base Information

Chemical Name:[closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]
CAS No.:82808-03-5
Molecular Formula:C₁₈H₃₃B₉NO₃P₂Rh
Molecular Weight:573.617
Hs Code.:

[closo-3,3-(dimethylphenylphosphine)2-3-NO<sub>3</sub>-3,1,2-RhC<sub>2</sub>B<sub>9</sub>H<sub>11</sub>]

Synonyms:[closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

Suppliers and Price of [closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

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Technology Process of [closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

There total 1 articles about [closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 82807-97-4
[closo-3-triphenylphosphine-3,3-nitrato-3,1,2-RhC₂B₉H₁₁]

: 672-66-2
Dimethyl(phenyl)phosphine

: 82808-03-5
[closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

Guidance literature:: In diethyl ether; byproducts: PPh3; under Ar, PMe2Ph added to stirred soln. of Rh complex in diethyl ether at room temp., mixt. stirred for 15 min; heptane added, diethyl ether removed in vac., ppt. filtered off in air,washed three times with heptane, dried by suction and in vac., elem. anal.;

Reference yield: 95.0%

: 82808-03-5
[closo-3,3-(dimethylphenylphosphine)2-3-NO₃-3,1,2-RhC₂B₉H₁₁]

: 89363-55-3
[closo-3,3-(PMe₂Ph)2-3-Cl-3,1,2-RhC₂B₉H₁₁]

Guidance literature:: With HCl; In tetrahydrofuran; under Ar, 37% HCl added to THF soln. of Rh complex, mixt. stirred for 15 min at room temp., further drops of HCl added, stirred for 75 min; heptane added, THF removed in vac., ppt. filtered off in air, washed with pentane, dried by suction;