4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide

Base Information

Chemical Name:4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide
CAS No.:87531-46-2
Molecular Formula:C₁₈H₂₇NO₂S
Molecular Weight:321.484
Hs Code.:

Synonyms:4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide

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Chemical Property of 4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide

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Technology Process of 4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide

There total 3 articles about 4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 123-72-8
butyraldehyde

: 87531-40-6
(E)-N-t-butyl-2-methyl-3-(phenylthio)propenamide

: 87531-46-2
4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1.) -80- -70 deg C, 1.5 h; 2.) -45- -25 deg C, 1.5 h;
DOI:10.1246/cl.1983.1065

Reference yield:

: 1078-67-7
(E)-2-Methyl-3-phenylsulfanyl-acryloyl chloride

: 87531-46-2
4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide

Guidance literature:: Multi-step reaction with 2 steps

2: 97 percent / LDA / tetrahydrofuran / 1.) -80- -70 deg C, 1.5 h; 2.) -45- -25 deg C, 1.5 h

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1246/cl.1983.1065

Reference yield:

: 2-Phenylsulfanylmethyl-acryloyl chloride

: 87531-46-2
4-Hydroxy-2-[1-phenylsulfanyl-meth-(E)-ylidene]-heptanoic acid tert-butylamide

Guidance literature:: Multi-step reaction with 2 steps

2: LDA / tetrahydrofuran / 1.) -80- -70 deg C, 1.5 h; 2.) -45- -25 deg C, 1.5 h

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1246/cl.1983.1065