8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile

Base Information

Chemical Name:8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile
CAS No.:113756-60-8
Molecular Formula:C₃₂H₂₅N₃O₅
Molecular Weight:531.568
Hs Code.:

Synonyms:8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile

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Chemical Property of 8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile

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Technology Process of 8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile

There total 1 articles about 8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 612-23-7
2-nitrobenzyl chloride

: 36547-83-8
2-benzoyl-8-benzyloxy-1,2-dihydro-7-methoxy-isoquinoline-1-carbonitrile

: 113756-60-8
8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile

Guidance literature:: for 2h;

Reference yield: 94.0%

: 113756-60-8
8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile

: 113756-65-3
8-benzyloxy-1-(2'-nitrobenzyl)-7-methoxyisoquinoline

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In methanol; for 24h; Ambient temperature;

Reference yield:

: 113756-60-8
8-benzyloxy-N-benzoyl-1-(2'-nitrobenzyl)-1,2-dihydro-7-methoxyisoquinoline-1-carbonitrile

: 1-(2'-diazobenzyl tetrafluoroborate)-7-methoxyisoquinolin-8-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / Triton B (40percent in water) / methanol / 24 h / Ambient temperature

2: 92 percent / hydrochloric acid, H₂ / 10percent Pd/C / ethanol / Ambient temperature

3: 84 percent / fluoroboric acid, isoamyl nitrite / propan-2-ol / 0.5 h / 0 - 5 °C

With hydrogenchloride; tetrafluoroboric acid; hydrogen; N-benzyl-trimethylammonium hydroxide; isopentyl nitrite; palladium on activated charcoal; In methanol; ethanol; isopropyl alcohol;