Technology Process of C29H52N5O7PS
There total 12 articles about C29H52N5O7PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
1,4-dioxane; water;
DOI:10.1039/c1ob05384a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetonitrile / 1 h / Inert atmosphere
2.1: trimethylphosphane / tetrahydrofuran / 4 h / Inert atmosphere
2.2: 0.5 h
3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere
4.1: sodium iodide / acetone / 36 h / Reflux; Inert atmosphere
5.1: trifluoroacetic acid / 1,4-dioxane; water
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium iodide; trimethylphosphane;
In
tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c1ob05384a
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran
2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / -40 °C / Inert atmosphere
3.1: acetonitrile / 1 h / Inert atmosphere
4.1: trimethylphosphane / tetrahydrofuran / 4 h / Inert atmosphere
4.2: 0.5 h
5.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere
6.1: sodium iodide / acetone / 36 h / Reflux; Inert atmosphere
7.1: trifluoroacetic acid / 1,4-dioxane; water
With
2,6-dimethylpyridine; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium iodide; trimethylphosphane;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c1ob05384a
