(^SiR,R)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-2-phenylethyl]-6-methylpyridine

Base Information

• Chemical Name: (^SiR,R)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-2-phenylethyl]-6-methylpyridine
• CAS No.: 1126532-45-3
• Molecular Formula: C₂₇H₃₃NOSi
• Molecular Weight: 415.651

Synonyms:(^SiR,R)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-2-phenylethyl]-6-methylpyridine

Chemical Property of (^SiR,R)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-2-phenylethyl]-6-methylpyridine

Chemical Property:

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Technology Process of (^SiR,R)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-2-phenylethyl]-6-methylpyridine

There total 1 articles about (^SiR,R)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-2-phenylethyl]-6-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

(SiS)-1-tert-butyl-1,2,3,4-tetrahydro-1-silanaphthalene (919513-39-6) + rac-1-phenyl-2-(6-methylpyridin-2-yl)ethanol (75792-98-2) → (S)-1-phenyl-2-(6-methylpyridin-2-yl)ethanol (1126532-63-5) + (SiR,R)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-2-phenylethyl]-6-methylpyridine (1126532-45-3)

Guidance literature:

With tris(3,5-dimethylphenyl)phosphine; copper(l) chloride; sodium t-butanolate; In toluene; at 20 ℃; for 24h; optical yield given as %ee; stereoselective reaction; Inert atmosphere;

DOI:10.1002/chem.200801377

upstream raw materials:

(SiS)-1-tert-butyl-1,2,3,4-tetrahydro-1-silanaphthalene

rac-1-phenyl-2-(6-methylpyridin-2-yl)ethanol

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