methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate

Base Information

• Chemical Name: methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate
• CAS No.: 1207373-44-1
• Molecular Formula: C₂₈H₂₇N₂O₄PS
• Molecular Weight: 518.573

Synonyms:methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate

Chemical Property of methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate

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Technology Process of methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate

There total 1 articles about methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-{[(2-azidophenyl)sulfonyl]amino}propanoate (1207374-17-1) + triphenylphosphine (603-35-0) → methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate (1207373-44-1)

Guidance literature:

In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.064

Reference yield: 93.0%

methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate (1207373-44-1) + benzyl isothiocyanate (3173-56-6) → methyl 3-[3-(benzylamino)-1,1-dioxido-2H-1,2,4-benzothiadiazin-2-yl]propanoate (1207373-76-9)

Guidance literature:

In toluene; at 110 ℃; for 15h; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.064

Reference yield: 87.0%

methyl 3-[({2-[(triphenylphosphoranyl)amino]phenyl}sulfonyl)amino]propanoate (1207373-44-1) + 4-Methoxyphenyl isocyanate (5416-93-3) → methyl 3-{3-[(4-methoxyphenyl)amino]-1,1-dioxido-2H-1,2,4-benzothiadiazin-2-yl}propanoate (1207373-74-7)

Guidance literature:

In toluene; at 110 ℃; for 2.5h; Inert atmosphere;

DOI:10.1016/j.tet.2009.11.064

upstream raw materials:

methyl 3-{[(2-azidophenyl)sulfonyl]amino}propanoate

triphenylphosphine

Downstream raw materials:

methyl 3-{3-[(4-chlorophenyl)amino]-1,1-dioxido-2H-1,2,4-benzothiadiazin-2-yl}propanoate

methyl 3-(3-anilino-1,1-dioxido-2H-1,2,4-benzothiadiazin-2-yl)propanoate

methyl 3-{3-[(4-methylphenyl)amino]-1,1-dioxido-2H-1,2,4-benzothiadiazin-2-yl}propanoate

methyl 3-{3-[(4-methoxyphenyl)amino]-1,1-dioxido-2H-1,2,4-benzothiadiazin-2-yl}propanoate

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