tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid)

Base Information

• Chemical Name: tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid)
• CAS No.: 1392413-73-8
• Molecular Formula: C₃₄H₂₀O₈S₄
• Molecular Weight: 684.792
• Mol file: 1392413-73-8.mol

Synonyms:tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid)

Chemical Property of tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid)

Chemical Property:

• Boiling Point: 890.4±65.0 °C(Predicted)
• PKA: 3.69±0.10(Predicted)
• Density: 1.616±0.06 g/cm3(Predicted)

Purity/Quality:

≥99% ^*data from raw suppliers

4,4',4'',4'''-([2,2'-Bi(1,3-dithiolylidene)]-4,4',5,5'-tetrayl)tetrabenzoicacid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid)

There total 2 articles about tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C42H36O8S4 (1356336-61-2) → tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid) (1392413-73-8)

Guidance literature:

With methanol; water; In tetrahydrofuran; for 12h; Inert atmosphere; Reflux; Alkaline conditions;

DOI:10.1021/ja3059827

Reference yield:

C38H28O8S4 → tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid) (1392413-73-8)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; water;

DOI:10.1039/c7ce00183e

Reference yield: 84.0%

manganese(II) nitrate hydrate + tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid) (1392413-73-8) + water (7732-18-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → Mn2(tetrathiafulvalene-3,4,5,6-tetrakis(4-benzoic acid)-H4)(H2O)2*(N,N-dimethylformamide)0.7(H2O)1.75

Guidance literature:

In ethanol; at 75 ℃; for 72h;

DOI:10.1021/ja512437u

upstream raw materials:

C₄₂H₃₆O₈S₄