C₄₈H₆₇ClO₁₁

Base Information

Chemical Name:C₄₈H₆₇ClO₁₁
CAS No.:1335098-32-2
Molecular Formula:C₄₈H₆₇ClO₁₁
Molecular Weight:855.506
Hs Code.:

C<sub>48</sub>H<sub>67</sub>ClO<sub>11</sub>

Synonyms:C₄₈H₆₇ClO₁₁

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Chemical Property of C₄₈H₆₇ClO₁₁

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Technology Process of C₄₈H₆₇ClO₁₁

There total 11 articles about C₄₈H₆₇ClO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335098-29-7
C₂₄H₃₄O₇

: 1335098-32-2
C₄₈H₆₇ClO₁₁

Guidance literature:: Multi-step reaction with 4 steps

1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 - 0 °C / Inert atmosphere

2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 3 h / 110 °C / Inert atmosphere

3: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 - 20 °C / Inert atmosphere

4: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; sodium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

With n-butyllithium; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 2,2'-azobis(isobutyronitrile); triphenyl-arsane; tri-n-butyl-tin hydride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; water; toluene; 4: alkyl-Suzuki cross-coupling;
DOI:10.1002/anie.201103270

Reference yield:

: 1335098-28-6
C₂₇H₄₄O₇Si

: 1335098-32-2
C₄₈H₆₇ClO₁₁

Guidance literature:: Multi-step reaction with 6 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

2: camphor-10-sulfonic acid / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

3: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 - 0 °C / Inert atmosphere

4: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 3 h / 110 °C / Inert atmosphere

5: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 - 20 °C / Inert atmosphere

6: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; sodium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

With n-butyllithium; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 2,2'-azobis(isobutyronitrile); triphenyl-arsane; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane; water; toluene; 6: alkyl-Suzuki cross-coupling;
DOI:10.1002/anie.201103270

Reference yield:

: (2S,3S,5R,7R,9R,10S,11R,15S)-2-(2-Benzyloxy-ethyl)-10-chloro-11-methoxy-15-methyl-9-vinyl-1,6,8-trioxa-dispiro[4.1.5.3]pentadecan-3-ol

: 1335098-32-2
C₄₈H₆₇ClO₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; sodium hydroxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triphenyl-arsane; sodium hydroxide; In tetrahydrofuran; water; 2: alkyl-Suzuki cross-coupling;
DOI:10.1002/anie.201103270