(1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol

Base Information

Chemical Name:(1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol
CAS No.:1196476-42-2
Molecular Formula:C₃₁H₄₀O₄Si
Molecular Weight:504.742
Hs Code.:

Synonyms:(1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol

Suppliers and Price of (1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol

There total 1 articles about (1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1196476-40-0
tert-butyl ((1S,5S)-2-((4-methoxybenzyloxy)methyl)-5-methylcyclopent-2-enyloxy)diphenylsilane

: 1196476-42-2
(1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol

Guidance literature:: tert-butyl ((1S,5S)-2-((4-methoxybenzyloxy)methyl)-5-methylcyclopent-2-enyloxy)diphenylsilane; With Thexylboran; In tetrahydrofuran; at -20 - 20 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 - 20 ℃; for 12h; diastereoselective reaction;
DOI:10.1021/ol902221y

Reference yield: 77.0%

: 1196476-42-2
(1S,2R,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanol

: 1196476-44-4
(2S,3S,4S)-3-(tert-butyldiphenylsilyloxy)-2-((4-methoxybenzyloxy)methyl)-4-methylcyclopentanone

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol902221y