Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate

Base Information

Chemical Name:Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate
CAS No.:133748-08-0
Molecular Formula:C₂₀H₁₉NO₆
Molecular Weight:369.374
Hs Code.:

Synonyms:Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate

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Chemical Property of Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate

Chemical Property:

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Technology Process of Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate

There total 7 articles about Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1026527-16-1
Methanesulfonic acid 1-benzo[1,3]dioxol-5-yl-5-oxo-pyrrolidin-3-ylmethyl ester

: 133748-08-0
Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; Yield given;
DOI:10.1016/0223-5234(94)90029-9

Reference yield:

: 97-65-4,25119-64-6
2-methylenesuccinic acid

: 133748-08-0
Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 91.3 percent / Heating

2: 91.5 percent / conc. H₂SO₄ / CH₂Cl₂ / Heating

3: 98.9 percent / NaBH₄, MeOH / tetrahydrofuran / Heating

4: Et₃N / CH₂Cl₂

5: K₂CO₃ / dimethylformamide / 80 °C

With methanol; sodium tetrahydroborate; sulfuric acid; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(94)90029-9

Reference yield:

: 14268-66-7
benzo[1,3]dioxolo-5-ylamine

: 133748-08-0
Methyl 4-[1-(3,4-methylenedioxyphenyl)-2-pyrrolidon-4-yl]methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 91.3 percent / Heating

2: 91.5 percent / conc. H₂SO₄ / CH₂Cl₂ / Heating

3: 98.9 percent / NaBH₄, MeOH / tetrahydrofuran / Heating

4: Et₃N / CH₂Cl₂

5: K₂CO₃ / dimethylformamide / 80 °C

With methanol; sodium tetrahydroborate; sulfuric acid; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(94)90029-9