N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Base Information

Chemical Name:N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine
CAS No.:1555939-28-0
Molecular Formula:C₃₆H₃₇N₅O
Molecular Weight:555.723
Hs Code.:

N<sub>1</sub>-(3-phenylbutanoyl)-N<sub>2</sub>-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Synonyms:N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Suppliers and Price of N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

There total 4 articles about N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 4593-90-2,772-17-8
3-phenylbutyric acid

: 1555938-77-6
N-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

: 1555939-28-0
N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Guidance literature:: With sodium hydride; 1,1'-carbonyldiimidazole; In tetrahydrofuran; mineral oil; at 20 - 35 ℃; for 6.75h; Inert atmosphere;
DOI:10.1039/c3md00245d

Reference yield:

: 1555938-57-2
N₁,N₂-bis(benzyloxycarbonyl)-N₁-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

: 1555939-28-0
N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / methanol / 3 h / 20 °C

2: sodium hydride; 1,1'-carbonyldiimidazole / tetrahydrofuran; mineral oil / 6.75 h / 20 - 35 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; sodium hydride; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1039/c3md00245d

Reference yield:

: 172499-78-4
3-[N-Triphenylmethyl-imidazol-2-yl]-propan-1-ol

: 1555939-28-0
N₁-(3-phenylbutanoyl)-N₂-[3-(1-trityl-1H-imidazol-2-yl)propyl]guanidine

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol / 3 h / 20 °C

3: sodium hydride; 1,1'-carbonyldiimidazole / tetrahydrofuran; mineral oil / 6.75 h / 20 - 35 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; sodium hydride; triphenylphosphine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1039/c3md00245d