N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine

Base Information

• Chemical Name: N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine
• CAS No.: 753025-09-1
• Molecular Formula: C₂₉H₃₆N₂O
• Molecular Weight: 428.618
• Mol file: 753025-09-1.mol

Synonyms:N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine

Chemical Property of N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine

Chemical Property:

Purity/Quality:

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Technology Process of N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine

There total 1 articles about N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3,5-di-tert-butyl-2-hydroxybenzaldehyde (37942-07-7) + (S,S)-1,2-diphenyl-1,2-diaminoethane (29841-69-8) → N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine (753025-09-1)

Guidance literature:

In dichloromethane; at 0 ℃; for 48h;

DOI:10.1016/j.jcat.2004.02.037

Reference yield: 89.0%

N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine (753025-09-1) + 5,5'-di-tert-butyl-6,6'-dihydroxy-3,3'-(propane-2,2-diyl)dibenzaldehyde (457658-13-8) → 5,5-(2',2'-dimethylpropane)-di-[(S,S)-{N-(3-tert-butylsalicylidine)-N'-(3',5'-di-tert-butylsalicylidine)}-1,2-diphenylethylene diamine]

Guidance literature:

In ethanol; dichloromethane; Heating;

DOI:10.1016/j.jcat.2004.02.037

Reference yield: 56.0%

N-(2-hydroxy-3,5-di-tert-butylbenzaldehyde)-1-amino-1,2-diphenylethaneimine (753025-09-1) + 5-[2-(4-{2-[4-(acetylthio)phenyl]ethynyl}phenyl)ethynyl]-3-tert-butylsalicylaldehyde (412300-38-0) → (1S,2S)-N-{5-[2-(4-{2-[4-(acetylthio)phenyl]ethynyl}phenyl)ethynyl]-3-tert-butylsalicylidene}-N'-(3,5-di-tert-butylsalicylidene)-1,2-diphenylethylenediamine

Guidance literature:

With 3 A molecular sieve; In chloroform-d1; for 24h;

DOI:10.1039/b104103g

upstream raw materials:

3,5-di-tert-butyl-2-hydroxybenzaldehyde

(S,S)-1,2-diphenyl-1,2-diaminoethane