5H-dibenzocyclohepten-5-one hydrazone

Base Information

Chemical Name:5H-dibenzocyclohepten-5-one hydrazone
CAS No.:61047-37-8
Molecular Formula:C₁₅H₁₂N₂
Molecular Weight:220.274
Hs Code.:

5H-dibenzo<a,d>cyclohepten-5-one hydrazone

Synonyms:5H-dibenzocyclohepten-5-one hydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5H-dibenzocyclohepten-5-one hydrazone

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Technology Process of 5H-dibenzocyclohepten-5-one hydrazone

There total 1 articles about 5H-dibenzocyclohepten-5-one hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2222-33-5
dibenzosuberenon

: 256-81-5
suberene

: 61047-37-8
5H-dibenzocyclohepten-5-one hydrazone

Guidance literature:: With hydrazinium sulfate; hydrazine; Yield given; Heating;
DOI:10.1021/ja00327a018

Reference yield:

: 61047-37-8
5H-dibenzocyclohepten-5-one hydrazone

: 2222-33-5
dibenzosuberenon

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium sulphate, yellow mercuric oxide, potassium hydroxide, Celite / 1.) diethyl ether, ethanol, 3 h, 2.) ethanol, diethyl ether, room temp., overnight

2: 82 percent / benzene / 8 h / Ambient temperature

3: 83 percent / water, hydrochloric acid / acetic acid / 1 h / Heating

With hydrogenchloride; potassium hydroxide; Celite; water; sodium sulfate; mercury(II) oxide; In acetic acid; benzene;