3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)

Base Information

Chemical Name:3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)
CAS No.:1310450-05-5
Molecular Formula:C₃₃H₃₈N₂O₂
Molecular Weight:494.677
Hs Code.:

Synonyms:3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)

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Chemical Property of 3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)

Chemical Property:

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Technology Process of 3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)

There total 2 articles about 3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 122-97-4
3-Phenyl-1-propanol

: 1310450-07-7
C₂₄H₂₈N₂O₂

: 1310450-05-5
3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)

Guidance literature:: With toluene-4-sulfonic acid; trifluoroacetic acid; In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo200692c

Reference yield:

: 3-(bis(4-methoxyphenyl)(3-phenylpropoxy)methyl)-N,N-dimethylaniline

: 1310450-05-5
3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)

Guidance literature:: Multi-step reaction with 2 steps

1: water-d2; [D₃]acetonitrile / 0.12 h / UV-irradiation

2: toluene-4-sulfonic acid; trifluoroacetic acid / toluene / 20 °C / Inert atmosphere

With toluene-4-sulfonic acid; trifluoroacetic acid; In water-d2; [D₃]acetonitrile; toluene;
DOI:10.1021/jo200692c

Reference yield:

: 1310450-05-5
3,3'-((4-methoxyphenyl)(3-phenylpropoxy)methylene)bis(N,N-dimethylaniline)

: 104-53-0
3-phenyl-propionaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: water-d2; [D₃]acetonitrile / 0.12 h / UV-irradiation

2: dichloromethane / 20 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4: d⁽⁴⁾-methanol / 0.2 h / UV-irradiation

With sodium hydride; In tetrahydrofuran; water-d2; dichloromethane; d⁽⁴⁾-methanol; [D₃]acetonitrile;
DOI:10.1021/jo200692c