Lithium-bis(diphenylphosphanyl)amid

Base Information

Chemical Name:Lithium-bis(diphenylphosphanyl)amid
CAS No.:73785-70-3
Molecular Formula:C₂₄H₂₀LiNP₂
Molecular Weight:391.318
Hs Code.:

Synonyms:Lithium-bis(diphenylphosphanyl)amid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Lithium-bis(diphenylphosphanyl)amid

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Technology Process of Lithium-bis(diphenylphosphanyl)amid

There total 1 articles about Lithium-bis(diphenylphosphanyl)amid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2960-37-4
Bis(diphenylphosphanyl)amine

: 73785-70-3
Lithium-bis(diphenylphosphanyl)amid

Guidance literature:: With n-butyllithium; In hexane; benzene; 1.) room temp., 3 h; 2.) reflux, 1 h;

Reference yield: 92.0%

: 73785-70-3
Lithium-bis(diphenylphosphanyl)amid

: 7646-79-9,14543-09-0,16413-89-1
cobalt(II) chloride

: 1.1.3.3.5.5.7.7.9.9.11.11-dodecaphenyl-2.4.8.10-tetraaza-6-cobalta-1.3.5.7.9.11-hexaphospha-6-spirotricyclo{5.3.1.0(6.8)}undecane

Guidance literature:: In toluene; byproducts: LiCl, Co, tris(diphenylphosphino)amine; addn. of anhyd. CoCl2 to a suspn. of LiN(PPh2)2 in toluene (under N2), refluxing and stirring for 5 h, pptn.; filtration, reducing filtrate in volume, crystn., recrystn. from hot toluene, drying in vacuo for 48 h; elem. anal.;

Reference yield: 80.0%

: 14243-64-2
triphenylphosphine gold(I)chloride

: 73785-70-3
Lithium-bis(diphenylphosphanyl)amid

: N((C₆H₅)2PAuP(C₆H₅)2)2N

Guidance literature:: In tetrahydrofuran; byproducts: LiCl, P(C6H5)3; exclusion of air and moisture; addn. of soln. of Li-compd. to soln. of Au-complex, pptn. after a few seconds, stirred for 1h at room temp.; filtered, washed (THF), dried (high-vac., 2 h); elem. anal.;