5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

Base Information

Chemical Name:5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)
CAS No.:152567-41-4
Molecular Formula:C₄₂H₄₂O₁₂
Molecular Weight:738.788
Hs Code.:

Synonyms:5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

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Chemical Property of 5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

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Technology Process of 5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

There total 5 articles about 5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 142746-73-4
5,5',5''-<1,3,5-benzoltriyltris(1,2-ethendiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

: 152567-41-4
5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

Guidance literature:: With hydrogen; palladium on activated charcoal; In toluene; at 50 ℃; for 4h; under 2250.2 Torr;

Reference yield: 99.0%

: 142746-73-4
C₄₂H₃₆O₁₂

: 152567-41-4
5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

Guidance literature:: With hydrogen; palladium on activated charcoal; In toluene; under 2250.2 Torr;

Reference yield:

: 42268-88-2
1,3-dimethyl 5-(bromomethyl)benzene-1,3-dicarboxylate

: 152567-41-4
5,5',5''-<1,3,5-benzoltriyltris(1,2-ethandiyl)>tris(1,3-benzoldicarbonsaeure-dimethylester)

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / CHCl₃ / 2 h / Heating

2: 64 percent / MeOLi / tetrahydrofuran / 12 h / 0 °C

3: 99 percent / H₂ / 5 percent Pd/C / toluene / 4 h / 50 °C / 2250.2 Torr

With lithium methanolate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; chloroform; toluene;