4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide

Base Information

Chemical Name:4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide
CAS No.:114920-22-8
Molecular Formula:C₂₂H₂₅NO₅
Molecular Weight:383.444
Hs Code.:

Synonyms:4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide

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Chemical Property of 4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide

Chemical Property:

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Technology Process of 4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide

There total 3 articles about 4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93-59-4
Perbenzoic acid

: 1616-49-5
4-ethyl-3-methyl-6,7-dimethoxy-1-(3,4-dimethoxyphenyl)isoquinoline

: 114920-22-8
4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide

Guidance literature:: With chloroform; at 0 - 10 ℃;
DOI:10.1021/ja01159a014

Reference yield:

: 15462-91-6
3-[2-(3,4-dimethoxybenzoyl)-4,5-dimethoxyphenyl]pentan-2-one

: 114920-22-8
4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide

Guidance literature:: With pyridine; ethanol; hydroxylamine hydrochloride;
DOI:10.1021/ja01159a014

Reference yield:

: 82005-37-6
1-ethyl-3-(3,4-dimethoxy-phenyl)-5,6-dimethoxy-2-methyl-indene

: 114920-22-8
4-ethyl-1-(3,4-dimethoxy-phenyl)-6,7-dimethoxy-3-methyl-isoquinoline-2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: CrO₃; acetic acid

2: sodium acetate; aqueous ethanol; hydroxylamine hydrochloride

With chromium(VI) oxide; ethanol; hydroxylamine hydrochloride; sodium acetate; acetic acid;
DOI:10.1021/jo01374a019