Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate

Base Information

Chemical Name:Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate
CAS No.:152530-80-8
Molecular Formula:C₁₇H₁₉NO₂
Molecular Weight:269.343
Hs Code.:

Synonyms:Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate

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Chemical Property of Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate

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Technology Process of Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate

There total 4 articles about Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 143207-36-7
Methyl 2-chloro-2-<1'-<<(1''-methylcyclopropyl)phenylmethylene>amino>cyclopropyl>acetate

: 152530-80-8
Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate

Guidance literature:: With triethylamine; lithium iodide; In isopropyl alcohol; at 85 - 90 ℃; for 120h;
DOI:10.1021/jo00075a047

Reference yield:

: 78104-88-8
1-Methylcyclopropancarbonsaeurenitril

: 152530-80-8
Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / diethyl ether / 2 h / Ambient temperature

2: methanol / 72 h / Ambient temperature

3: 65 percent / LiI, Et₃N / propan-2-ol / 120 h / 85 - 90 °C

With triethylamine; lithium iodide; In methanol; diethyl ether; isopropyl alcohol;
DOI:10.1021/jo00075a047

Reference yield:

: 143207-33-4
(1-methyl-cyclopropyl)-phenyl ketone-imine

: 152530-80-8
Methyl 2-<<(1'-methylcyclopropyl)phenylmethylene>amino>cyclobutene-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 72 h / Ambient temperature

2: 65 percent / LiI, Et₃N / propan-2-ol / 120 h / 85 - 90 °C

With triethylamine; lithium iodide; In methanol; isopropyl alcohol;
DOI:10.1021/jo00075a047