octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside

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Chemical Name:octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside
CAS No.:848436-94-2
Molecular Formula:C₃₇H₄₈O₁₃
Molecular Weight:700.78
Hs Code.:

Synonyms:octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside

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Chemical Property of octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside

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Technology Process of octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside

There total 5 articles about octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: p-tolyl 2,5-di-O-acetyl-3-O-methyl-1-thio-D-arabinofuranoside

: 329360-19-2
octyl 2,3-di-O-benzoyl-α-D-arabinofuranoside

: 848436-94-2
octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.0833333h;
DOI:10.1016/j.bmc.2004.11.003

Reference yield:

: 848437-18-3
methyl 2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranoside

: 848436-94-2
octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂SO₄ / 1 h / 0 °C

2: 80 percent / BF₃-OEt₂ / CH₂Cl₂ / 0 - 20 °C

3: 71 percent / N-iodosuccinimide; silver(I) triflate / CH₂Cl₂ / 0.08 h / 0 °C

With N-iodo-succinimide; sulfuric acid; boron trifluoride diethyl etherate; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1016/j.bmc.2004.11.003

Reference yield:

: 1,2,5-tri-O-acetyl-3-O-methyl-D-arabinofuranose

: 848436-94-2
octyl 5-O-(2,5-di-O-acetyl-3-O-methyl-α-D-arabinofuranosyl)-2,3-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / BF₃-OEt₂ / CH₂Cl₂ / 0 - 20 °C

2: 71 percent / N-iodosuccinimide; silver(I) triflate / CH₂Cl₂ / 0.08 h / 0 °C

With N-iodo-succinimide; boron trifluoride diethyl etherate; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1016/j.bmc.2004.11.003