2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Base Information

Chemical Name:2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose
CAS No.:1203588-94-6
Molecular Formula:C₄₂H₄₈N₄O₁₀
Molecular Weight:768.864
Hs Code.:

Synonyms:2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

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Chemical Property of 2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

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Technology Process of 2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

There total 7 articles about 2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1203588-93-5
tert-butyldimethylsilyl 2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 1203588-94-6
2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 - 50 ℃;
DOI:10.1007/s00706-009-0172-0

Reference yield:

: 1203582-46-0
tert-butyldimethylsilyl (4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1→4)-2-deoxy-3,6-di-O-benzyl-2-phthalimido-β-D-glucopyranoside

: 1203588-94-6
2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: ethylenediamine / butan-1-ol / 0 - 90 °C

2: pyridine / 0 - 20 °C

3: methanol; sodium methylate / 0 - 20 °C

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 50 °C

With pyridine; methanol; tetrabutyl ammonium fluoride; sodium methylate; acetic acid; ethylenediamine; In tetrahydrofuran; butan-1-ol;
DOI:10.1007/s00706-009-0172-0

Reference yield:

: C₄₈H₆₂N₄O₁₀Si

: 1203588-94-6
2-acetamido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C

2: methanol; sodium methylate / 0 - 20 °C

3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 50 °C

With pyridine; methanol; tetrabutyl ammonium fluoride; sodium methylate; acetic acid; In tetrahydrofuran;
DOI:10.1007/s00706-009-0172-0