3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

Base Information

Chemical Name:3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile
CAS No.:692744-40-4
Molecular Formula:C₃₀H₂₆N₂O₄S₇
Molecular Weight:703.009
Hs Code.:

3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-<i>d</i>][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

Synonyms:3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

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Chemical Property of 3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

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Technology Process of 3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

There total 1 articles about 3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 158871-28-4
4,5-bis(2-cyanoethylthio)-1,3-dithiol-2-one

: 4,6-bis(2,4-dimethoxyphenyl)thieno[3,4-d][1,3]dithiole-2-thione

: 692744-40-4
3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

Guidance literature:: With phosphorous acid trimethyl ester; In toluene; at 80 ℃; for 12h;
DOI:10.1016/j.tetlet.2004.02.003

Reference yield:

: 692744-40-4
3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

: 2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-[1,3]dithiole-4,5-dithiol

Guidance literature:: With cesium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2004.02.003

Reference yield:

: 692744-40-4
3-[2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5-(2-cyano-ethylsulfanyl)-[1,3]dithiol-4-ylsulfanyl]-propionitrile

: 2-[4,6-bis-(2,4-dimethoxy-phenyl)-thieno[3,4-d][1,3]dithiol-2-ylidene]-5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiine

Guidance literature:: Multi-step reaction with 2 steps

1: CsOH / tetrahydrofuran

With cesium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2004.02.003