(S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester

Base Information

Chemical Name:(S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester
CAS No.:478404-14-7
Molecular Formula:C₂₆H₂₈N₂O₇S
Molecular Weight:512.584
Hs Code.:

Synonyms:(S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester

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Chemical Property of (S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester

Chemical Property:

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Technology Process of (S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester

There total 3 articles about (S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89979-13-5
benzyl N-chlorosulfonylcarbamate

: (S)-2-benzyl-3-(N-benzyloxy)aminopropanoic acid methyl ester hydrochloride

: 478404-14-7
(S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 6h;
DOI:10.1021/jm020258v

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 478404-14-7
(S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / 0 °C

2: NEt₃ / CH₂Cl₂ / 6 h

With triethylamine; In dichloromethane;
DOI:10.1021/jm020258v

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 478404-14-7
(S)-2-benzyl-3-(N-benzyloxy-N-(N-benzyloxycarbonyl)sulfamoyl)aminopropanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / 0 °C

2: triethylamine / CH₂Cl₂ / 6 h / 20 °C

With triethylamine; In dichloromethane;
DOI:10.1016/j.bmc.2004.02.012