methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside

Base Information

• Chemical Name: methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside
• CAS No.: 78468-56-1
• Molecular Formula: C₁₆H₂₁NO₆
• Molecular Weight: 323.346

Synonyms:methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside

Chemical Property of methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside

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Technology Process of methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside

There total 7 articles about methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

((2R,4aR,6S,8S,8aR)-8-Hydroxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-acetonitrile (78513-02-7) → methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside (78468-56-1)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; In ethanol; for 0.666667h;

DOI:10.1021/ja00405a027

Reference yield: 83.0%

((2R,4aR,6S,8R,8aR)-8-Hydroxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-acetic acid hydrazide → methyl 4,6-O-benzylidene-2-deoxy-3-C-<(aminocarbonyl)methyl>-α-D-ribo-hexopyranoside (78468-56-1)

Guidance literature:

With potassium hexacyanoferrate(VI);

DOI:10.1021/ja00405a027

Reference yield: 77.0%

((2R,4aR,6S,8S,8aR)-8-Hydroxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-acetic acid hydrazide → 2-((2R,4aR,6S,8S,8aR)-8-Hydroxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-acetamide (78468-56-1,78468-59-4)

Guidance literature:

With potassium hexacyanoferrate(VI);

DOI:10.1021/ja00405a027

upstream raw materials:

((2R,4aR,6S,8S,8aR)-8-Hydroxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl)-acetonitrile

methyl 4,6-O-(R)-benzylidene-2-deoxy-α-D-erythrohexopyranosid-3-ulose

methyl 4,6-O-benzylidene-2-deoxy-3-C-<(ethoxycarbonyl)methyl>-α-D-ribo-hexopyranoside

methyl 4,6-O-benzylidene-2-deoxy-3-C-<(ethoxycarbonyl)methyl>-α-D-arabino-hexopyranoside

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