C₃₁H₃₅N₅O₇

Base Information

Chemical Name:C₃₁H₃₅N₅O₇
CAS No.:1590380-77-0
Molecular Formula:C₃₁H₃₅N₅O₇
Molecular Weight:589.648
Hs Code.:

C<sub>31</sub>H<sub>35</sub>N<sub>5</sub>O<sub>7</sub>

Synonyms:C₃₁H₃₅N₅O₇

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Chemical Property of C₃₁H₃₅N₅O₇

Chemical Property:

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Technology Process of C₃₁H₃₅N₅O₇

There total 16 articles about C₃₁H₃₅N₅O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

: 1590380-76-9
C₃₈H₄₁N₅O₇

: 1590380-77-0
C₃₁H₃₅N₅O₇

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; for 1h; under 760.051 Torr;
DOI:10.1021/ol5002126

Reference yield:

: 15136-29-5
(S)-methyl 2-((S)-2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)propanoate

: 1590380-77-0
C₃₁H₃₅N₅O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 8 h / 0 - 20 °C / Inert atmosphere

3.1: lithium hydroxide / water; tetrahydrofuran; methanol / 1 h / 0 - 20 °C / Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

4.2: 8 h / 0 - 20 °C / Inert atmosphere

5.1: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine; pentafluorophenyl diphenyl-phosphinate / acetonitrile / 24.5 h / -5 - 20 °C / Inert atmosphere

7.1: lithium hydroxide / water; tetrahydrofuran; methanol / 1 h / 0 - 20 °C / Inert atmosphere

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

8.2: 8 h / 0 - 20 °C / Inert atmosphere

9.1: hydrogen; palladium on activated charcoal / methanol / 1 h / 760.05 Torr

With palladium on activated charcoal; pentafluorophenyl diphenyl-phosphinate; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ol5002126

Reference yield:

: 1401236-31-4
Boc-Phe-Phe-Ala-OH

: 1590380-77-0
C₃₁H₃₅N₅O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

1.2: 8 h / 0 - 20 °C / Inert atmosphere

2.1: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; pentafluorophenyl diphenyl-phosphinate / acetonitrile / 24.5 h / -5 - 20 °C / Inert atmosphere

4.1: lithium hydroxide / water; tetrahydrofuran; methanol / 1 h / 0 - 20 °C / Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

5.2: 8 h / 0 - 20 °C / Inert atmosphere

6.1: hydrogen; palladium on activated charcoal / methanol / 1 h / 760.05 Torr

With palladium on activated charcoal; pentafluorophenyl diphenyl-phosphinate; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ol5002126