(4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane

Base Information

Chemical Name:(4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane
CAS No.:1026024-01-0
Molecular Formula:C₃₂H₄₉O₇P
Molecular Weight:576.711
Hs Code.:

Synonyms:(4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane

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Chemical Property of (4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane

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Technology Process of (4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane

There total 2 articles about (4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1517-69-7
(R)-1-phenylethanol

: 1026023-96-0
(4R,5R)-bis((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl) 2-chloro-1,3,2-dioxaphospholane-4,5-dicarboxylate

: 1026024-01-0
(4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane

Guidance literature:: With triethylamine; In tetrahydrofuran; at 25 ℃; for 2h;
DOI:10.1021/jo7026068

Reference yield:

: 77302-56-8,1287683-04-8
(+)-(R,R)-Weinsaeure-di<(-)-(1R,2S,5R)-menthyl>ester

: 1026024-01-0
(4R,5R)-bis[(1R,2S,5R)-menth-1-yloxycarbonyl]-2-[(R)-1-phenyleth-1-yloxy]-1,3,2-dioxaphospholane

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride / tetrahydrofuran / 1 h / 65 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran; chloroform-d1 / 20 °C

With triethylamine; phosphorus trichloride; In tetrahydrofuran; chloroform-d1;
DOI:10.1016/j.tetasy.2011.04.004