2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide

Base Information

Chemical Name:2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide
CAS No.:139983-97-4
Molecular Formula:C₂₂H₁₇Cl₂N₅O₂
Molecular Weight:454.315
Hs Code.:

Synonyms:2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide

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Chemical Property of 2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide

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Technology Process of 2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide

There total 4 articles about 2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 77423-12-2
6,7-dichloro-1,2-dihydro-3,1-benzoxazine-2,4-dione

: 2-amino<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>ethanone hydrochloride

: 139983-97-4
2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide

Guidance literature:: In water; Ambient temperature;
DOI:10.1021/jm00018a011

Reference yield:

: 122957-08-8
ethyl 4'-(2-methylimidazo[4,5-c]pyridin-1-yl)benzoylacetate

: 139983-97-4
2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / aq. NaNO₂ / acetic acid / 1.5 h / 5 °C

2: 94 percent / H₂ / 5percent Pd/C / acetic acid / 5 h / 30 °C / 2585.7 Torr

3: 2M aq. HCl / 3 h / Heating

4: 45 percent / H₂O / Ambient temperature

With hydrogenchloride; hydrogen; sodium nitrite; palladium on activated charcoal; In water; acetic acid;
DOI:10.1021/jm00018a011

Reference yield:

: ethyl 4'-(2-methylimidazo<4,5-c>pyrid-1-yl)benzoyloximidoacetate

: 139983-97-4
2-amino-4,5-dichloro-N-<2-<4-(2-methylimidazo<4,5-c>pyrid-1-yl)phenyl>-2-oxoethyl>benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / H₂ / 5percent Pd/C / acetic acid / 5 h / 30 °C / 2585.7 Torr

2: 2M aq. HCl / 3 h / Heating

3: 45 percent / H₂O / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In water; acetic acid;
DOI:10.1021/jm00018a011