(1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol

Base Information

• Chemical Name: (1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol
• CAS No.: 1469904-18-4
• Molecular Formula: C₁₀H₁₅ClO
• Molecular Weight: 186.681
• Mol file: 1469904-18-4.mol

Synonyms:(1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol

Chemical Property of (1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of (1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol

There total 1 articles about (1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

(1R,2R,6S)-3-methyl-6-(1-methylethenyl)cyclohex-3-ene-1,2-diol (935670-67-0) → (1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol (1469904-18-4) + (1S,4R,6S)-4-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-2-enol (1469904-19-5)

Guidance literature:

With methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In toluene; for 3h; Reflux;

DOI:10.2174/1573406411309050013

Reference yield: 50.0%

(1R,2R,6S)-2-chloro-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol (1469904-18-4) → (1S,6S)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol (122621-70-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 6h;

DOI:10.2174/1573406411309050013

upstream raw materials:

(1R,2R,6S)-3-methyl-6-(1-methylethenyl)cyclohex-3-ene-1,2-diol

Downstream raw materials:

(1S,6S)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-enol