p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate

Base Information

Chemical Name:p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate
CAS No.:65075-37-8
Molecular Formula:C₁₅H₁₅N₅O₉S
Molecular Weight:441.378
Hs Code.:

Synonyms:p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate

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Chemical Property of p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate

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Technology Process of p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate

There total 4 articles about p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 192517-68-3
p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-2',2'-diethoxypropionate

: 65075-37-8
p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate

Guidance literature:: With trifluoroacetic acid; at 50 ℃; for 1h;
DOI:10.1039/a700650k

Reference yield:

: (3S,4S)-3-azido-1-<2',2'-diethoxy-1'-(p-nitrobenzylcarbamoyl)ethyl>-4-(hydroxymethyl)azetidin-2-one

: 65075-37-8
p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran / 1 h / Ambient temperature

2: N₂O₄, NaOAc / CHCl₃ / 1 h / 0 °C

3: CCl₄ / 3 h / Heating

4: 81 percent / 95percent aq. TFA / 1 h / 50 °C

With sodium acetate; dinitrogen tetraoxide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; tetrachloromethane; chloroform;
DOI:10.1039/a700650k

Reference yield:

: C₁₉H₂₅N₇O₁₀S

: 65075-37-8
p-nitrobenzyl 2'-<(2S,3S)-3-azido-2-methylsulfonyloxymethyl-4-oxoazetidin-1-yl>-3'-hydroxypropenoate

Guidance literature:: Multi-step reaction with 2 steps

1: CCl₄ / 3 h / Heating

2: 81 percent / 95percent aq. TFA / 1 h / 50 °C

With trifluoroacetic acid; In tetrachloromethane;
DOI:10.1039/a700650k