Technology Process of C47H65N3O11
There total 8 articles about C47H65N3O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; potassium hydroxide;
In
methanol;
for 72h;
Reflux;
DOI:10.1021/ol4021207
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 0 - 20 °C
2: palladium 10% on activated carbon; hydrogen; hydrazine / dichloromethane; methanol / 1.5 h / 20 °C / 3375.34 Torr
3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
4: potassium hydroxide; water / methanol / 72 h / Reflux
With
palladium 10% on activated carbon; water; hydrogen; triethylamine; potassium hydroxide; hydrazine;
In
methanol; dichloromethane;
DOI:10.1021/ol4021207
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide; water / methanol / 24 h / 60 °C
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
3: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
4: potassium hydroxide; water / methanol / 72 h / Reflux
With
oxalyl dichloride; water; triethylamine; N,N-dimethyl-formamide; potassium hydroxide;
In
methanol; dichloromethane;
DOI:10.1021/ol4021207