4,4'-(α,α'-dibromo)tolylpyridine

Base Information

• Chemical Name: 4,4'-(α,α'-dibromo)tolylpyridine
• CAS No.: 717832-46-7
• Molecular Formula: C₁₂H₉Br₂N
• Molecular Weight: 327.018
• Mol file: 717832-46-7.mol

Synonyms:4,4'-(α,α'-dibromo)tolylpyridine

Chemical Property of 4,4'-(α,α'-dibromo)tolylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4,4'-(α,α'-dibromo)tolylpyridine

There total 1 articles about 4,4'-(α,α'-dibromo)tolylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(p-tolyl)pyridine (4423-10-3) → 4,4'-(α,α'-dibromo)tolylpyridine (717832-46-7)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 16h; Heating;

DOI:10.1002/chem.200305570

Reference yield: 54.0%

C75H112O8 (143018-00-2) + 4,4'-(α,α'-dibromo)tolylpyridine (717832-46-7) → C87H119NO8

Guidance literature:

With potassium carbonate; In N,N-dimethyl acetamide; at 80 ℃; for 16h;

DOI:10.1002/chem.200401061

Reference yield: 53.0%

C84H118O8P2S2 + 4,4'-(α,α'-dibromo)tolylpyridine (717832-46-7) → C108H132N2O8P2S2

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 19h; optical yield given as %de; Sealed tube;

DOI:10.1002/ejoc.201001668

upstream raw materials:

4-(p-tolyl)pyridine