N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester

Base Information

Chemical Name:N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester
CAS No.:219686-75-6
Molecular Formula:C₂₉H₄₈N₂O₈
Molecular Weight:552.709
Hs Code.:

Synonyms:N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester

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Chemical Property of N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester

Chemical Property:

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Technology Process of N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester

There total 3 articles about N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 219686-75-6
N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / methanol / 1 h / 50 °C

2: 86 percent / NaBH₄ / ethanol / 2 h / 50 °C

3: 60 percent / 6 M aq. HCl / 8 h / Heating

4: 75 percent / Et₃N / dimethylformamide / 2 h / 60 °C

With hydrogenchloride; sodium tetrahydroborate; triethylamine; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja981123a

Reference yield:

: 219686-72-3
N-(3,5-dimethoxybenzylidene)-N'-acetylethylenediamine

: 219686-75-6
N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / NaBH₄ / ethanol / 2 h / 50 °C

2: 60 percent / 6 M aq. HCl / 8 h / Heating

3: 75 percent / Et₃N / dimethylformamide / 2 h / 60 °C

With hydrogenchloride; sodium tetrahydroborate; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja981123a

Reference yield:

: 219686-73-4
N-(3,5-dimethoxybenzyl)-N'-acetylethylenediamine

: 219686-75-6
N-(3,5-dimethoxybenzyl)ethylenediamine N,N',N'-triacetic acid tri-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / 6 M aq. HCl / 8 h / Heating

2: 75 percent / Et₃N / dimethylformamide / 2 h / 60 °C

With hydrogenchloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja981123a