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Technology Process of [Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2)

[Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2)

Base Information
  • Chemical Name:[Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2)
  • CAS No.:1092078-31-3
  • Molecular Formula:C29H31ClN3O7Pd*C102H121N4O2
  • Molecular Weight:2110.56
  • Hs Code.:
[Pd(Cl)NC<sub>5</sub>H<sub>3</sub>(NCOCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>O<sub>2</sub>C<sub>4</sub>H<sub>8</sub>)2O]<sup>(1-)</sup>*C<sub>5</sub>H<sub>4</sub>NCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>C<sub>6</sub>H<sub>12</sub>(C<sub>2</sub>HN<sub>3</sub>)(C<sub>3</sub>H<sub>6</sub>OC<sub>6</sub>H<sub>4</sub>C<sub>31</sub>H<sub>39</sub>)2<sup>(1+)</sup>=[PdClC<sub>29</sub>H<sub>31</sub>N<sub>3</sub>O<sub>7</sub>](C<sub>102</sub>H<sub>121</sub>N<sub>4</sub>O<sub>2</sub>)

Synonyms:[Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2)

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Chemical Property of [Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2)
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Technology Process of [Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2)

There total 1 articles about [Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1-(3-azido-propoxy)-4-(tris-(4-tert-butyl-phenyl)methyl)benzene
876400-54-3

1-(3-azido-propoxy)-4-(tris-(4-tert-butyl-phenyl)methyl)benzene

[palladium(acetonitrile)NC<sub>5</sub>H<sub>3</sub>(N(CO)CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>(OCH<sub>2</sub>CH<sub>2</sub>)2)2O]
832082-08-3

[palladium(acetonitrile)NC5H3(N(CO)CH2C6H4(OCH2CH2)2)2O]

(C<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)3CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)3C<sub>5</sub>H<sub>4</sub>NCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CC(CH<sub>2</sub>)6CCH<sup>(1+)</sup>*Cl<sup>(1-)</sup>=((C<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)3CC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)3C<sub>5</sub>H<sub>4</sub>NCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CC(CH<sub>2</sub>)6CCH)Cl
1092078-29-9

(C6H4C(CH3)3)3CC6H4O(CH2)3C5H4NCH2C6H4CC(CH2)6CCH(1+)*Cl(1-)=((C6H4C(CH3)3)3CC6H4O(CH2)3C5H4NCH2C6H4CC(CH2)6CCH)Cl

[Pd(Cl)NC<sub>5</sub>H<sub>3</sub>(NCOCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>O<sub>2</sub>C<sub>4</sub>H<sub>8</sub>)2O]<sup>(1-)</sup>*C<sub>5</sub>H<sub>4</sub>NCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>C<sub>6</sub>H<sub>12</sub>(C<sub>2</sub>HN<sub>3</sub>)(C<sub>3</sub>H<sub>6</sub>OC<sub>6</sub>H<sub>4</sub>C<sub>31</sub>H<sub>39</sub>)2<sup>(1+)</sup>=[PdClC<sub>29</sub>H<sub>31</sub>N<sub>3</sub>O<sub>7</sub>](C<sub>102</sub>H<sub>121</sub>N<sub>4</sub>O<sub>2</sub>)
1092078-31-3

[Pd(Cl)NC5H3(NCOCH2C6H4O2C4H8)2O](1-)*C5H4NCH2C6H4C2C6H12(C2HN3)(C3H6OC6H4C31H39)2(1+)=[PdClC29H31N3O7](C102H121N4O2)

Guidance literature:
With tetrakis(actonitrile)copper(I) hexafluorophosphate; tris(benzyltriazolylmethyl)amine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile; ((C6H4C4H9)3CC6H4O(CH2)3C5H4NCH2C6H4CC(CH2)6CCH)Cl and Pd complex soln. (CH2Cl2) stirred (1 h), (C6H4C4H9)3CC6H4O(CH2)3N3 (1.1 equiv.) and iPr2EtN (1 equiv.) added, Cu(CH3CN)4PF4 and tris(benzyltriazolylmethyl)amine soln. (CH3CN) added, stirred (18 h); volatiles removed (under vac.), residue taken up in CH2Cl2, soln. washedwith satd. NH4Cl, aq. phase reextracted with CH2Cl2, combined organic e xtracts concd. (under vac.), subjected to flash chromy. on silica gel (0-3% MeOH in CH2Cl2 as eluent);
DOI:10.1002/anie.200802745
upstream raw materials:

1-(3-azido-propoxy)-4-(tris-(4-tert-butyl-phenyl)methyl)benzene

[palladium(acetonitrile)NC5H3(N(CO)CH2C6H4(OCH2CH2)2)2O]

(C6H4C(CH3)3)3CC6H4O(CH2)3C5H4NCH2C6H4CC(CH2)6CCH(1+)*Cl(1-)=((C6H4C(CH3)3)3CC6H4O(CH2)3C5H4NCH2C6H4CC(CH2)6CCH)Cl

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