2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

Base Information

Chemical Name:2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester
CAS No.:195324-03-9
Molecular Formula:C₂₄H₂₆N₂O₅
Molecular Weight:422.481
Hs Code.:

Synonyms:2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

Suppliers and Price of 2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

There total 5 articles about 2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-Oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

: 195324-03-9
2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

Guidance literature:: With triethylamine; Methanesulfonyl azide; In tetrahydrofuran; for 20h; Yield given;
DOI:10.1021/ja971687z

Reference yield:

: 612-14-6
phthalyl alcohol

: 195324-03-9
2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH / 1.) THF, 0 deg C, 15 min, 2) THF, from 0 deg C to room temperature, overnight.

2: 97 percent / Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

3: 1.) NaH / 1.) THF, room temperature, 15 min, 2.) 20 h.

4: Et₃N / tetrahydrofuran / 20 h / 0 °C

5: methanesulfonyl azide, Et₃N / tetrahydrofuran / 20 h

With sodium hydride; triethylamine; Methanesulfonyl azide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja971687z

Reference yield:

: 195323-87-6
2-(2-methyl-2-propen-1-yloxymethyl)benzyl alcohol

: 195324-03-9
2-Diazo-3-oxo-butyric acid 2-[2-(2-methyl-allyloxymethyl)-benzyloxymethyl]-benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

2: 1.) NaH / 1.) THF, room temperature, 15 min, 2.) 20 h.

3: Et₃N / tetrahydrofuran / 20 h / 0 °C

4: methanesulfonyl azide, Et₃N / tetrahydrofuran / 20 h

With sodium hydride; triethylamine; Methanesulfonyl azide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja971687z