[(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

Base Information

Chemical Name:[(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol
CAS No.:406684-10-4
Molecular Formula:C₂₂H₃₀O₂Si
Molecular Weight:354.565
Hs Code.:

Synonyms:[(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

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Chemical Property of [(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

Chemical Property:

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Technology Process of [(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

There total 4 articles about [(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₄₄O₂Si₂

: 406684-10-4
[(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

Guidance literature:: camphor-10-sulfonic acid; In methanol; at 0 ℃; for 0.666667h;
DOI:10.1002/1521-3773(20020104)41:1<176::AID-ANIE176>3.0.CO;2-#

Reference yield:

: 153618-35-0
menthyl (1S,2S,3S)-2-hydroxymethyl-3-methylcyclopropane-1-carboxylate

: 406684-10-4
[(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

Guidance literature:: Multi-step reaction with 4 steps

1: imidazole / CH₂Cl₂ / 0.5 h / 20 °C

2: LiAlH₄ / diethyl ether / 1 h / 0 °C

3: imidazole / CH₂Cl₂ / 1 h / 20 °C

4: camphorsulfonic acid / methanol / 0.67 h / 0 °C

With 1H-imidazole; lithium aluminium tetrahydride; camphor-10-sulfonic acid; In methanol; diethyl ether; dichloromethane;
DOI:10.1002/1521-3773(20020104)41:1<176::AID-ANIE176>3.0.CO;2-#

Reference yield:

: [(1S,2S,3R)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

: 406684-10-4
[(1S,2S,3S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methyl-cyclopropyl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / CH₂Cl₂ / 1 h / 20 °C

2: camphorsulfonic acid / methanol / 0.67 h / 0 °C

With 1H-imidazole; camphor-10-sulfonic acid; In methanol; dichloromethane;
DOI:10.1002/1521-3773(20020104)41:1<176::AID-ANIE176>3.0.CO;2-#