N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide

Base Information

Chemical Name:N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide
CAS No.:740873-24-9
Molecular Formula:C₂₂H₃₈N₄O₂S
Molecular Weight:422.635
Hs Code.:

Synonyms:N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide

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Technology Process of N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide

There total 6 articles about N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 740873-23-8
C-cyclohexyl-N-methyl-N-{4-[4-(3-nitrophenyl)piperazin-1-yl]butyl}methanesulfonamide

: 740873-24-9
N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide

Guidance literature:: With hydrogenchloride; tin(ll) chloride; In methanol; at -10 - 20 ℃;
DOI:10.1021/jm0508641

Reference yield:

: 54054-85-2
1-(3-nitrophenyl)piperazine

: 740873-24-9
N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Et₃N / tetrahydrofuran / 48 h / 20 °C

2: 76 percent / SnCl₂; aq. HCl / methanol / -10 - 20 °C

With hydrogenchloride; triethylamine; tin(ll) chloride; In tetrahydrofuran; methanol;
DOI:10.1021/jm0508641

Reference yield:

: cyclohexylmethanesulfonic acid 4-(cyclohexylmethanesulfonylmethylamino)butyl ester

: 740873-24-9
N-{4-[4-(3-aminophenyl)piperazin-1-yl]butyl}-C-cyclohexyl-N-methylmethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Et₃N / tetrahydrofuran / 48 h / 20 °C

2: 76 percent / SnCl₂; aq. HCl / methanol / -10 - 20 °C

With hydrogenchloride; triethylamine; tin(ll) chloride; In tetrahydrofuran; methanol;
DOI:10.1021/jm0508641