benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate

Base Information

Chemical Name:benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate
CAS No.:94820-98-1
Molecular Formula:C₃₃H₃₆O₉
Molecular Weight:576.643
Hs Code.:

Synonyms:benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate

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Chemical Property of benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate

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Technology Process of benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate

There total 2 articles about benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1133162-86-3
benzyl 4-O-benzoyl-2,6-dideoxy-2-(p-tolylthio)-β-D-glucopyranosyl-(1->3)-4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranoside

: 94820-98-1
benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 105 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo900131a

Reference yield: 23.0%

: 86448-03-5
C₃₄H₃₄Br₂O₁₀

: 94820-97-0
benzyl 4-O-benzoyl-3-O-(3-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,3'-dibenzoate

: 94820-98-1
benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In 1,2-dimethoxyethane; for 24h; Ambient temperature;
DOI:10.1021/jo00207a009

Reference yield:

: 1133162-80-7
1,5-anhydro-3-O-(tert-butyldimethylsilyl)-4-O-isobutyryl-1,2,6-trideoxy-3-C-methyl-L-arabino-hex-1-enitol

: 94820-98-1
benzyl 4-O-benzoyl-3-O-(4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl)-2,6-dideoxy-β-D-arabino-hexopyranoside 4,4'-dibenzoate

: 1133162-93-2
benzyl 3-O-(tert-butyldimethylsilyl)-4-O-isobutyryl-2,6-dideoxy-2-iodo-3-C-methyl-α-L-mannopyranosyl-(1->3)-4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl-(1->3)-4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranoside

: benzyl 3-O-(tert-butyldimethylsilyl)-4-O-isobutyryl-2,6-dideoxy-2-iodo-3-C-methyl-β-L-mannopyranosyl-(1->3)-4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranosyl-(1->3)-4-O-benzoyl-2,6-dideoxy-β-D-arabino-hexopyranoside

Guidance literature:: With N-iodo-succinimide; In dichloromethane; at 20 ℃; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1021/jo900131a