2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine

Base Information

Chemical Name:2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine
CAS No.:1421689-41-9
Molecular Formula:C₁₇H₂₃N
Molecular Weight:246.337
Hs Code.:

2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D<sub>5</sub>]-phenylazetidine

Synonyms:2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine

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Chemical Property of 2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine

Chemical Property:

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Technology Process of 2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine

There total 4 articles about 2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1421689-88-4
4-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidin-2-one

: 1421689-41-9
2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine

Guidance literature:: 4-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidin-2-one; With aluminum (III) chloride; lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

With ethylenediaminetetraacetic acid; In tetrahydrofuran; water; for 0.5h; Inert atmosphere;
DOI:10.1021/ol303518n

Reference yield:

: 1421689-74-8
3-hydroxy-N-[2,3,4,5,6-D₅]-phenylundec-4-ynamide

: 1421689-41-9
2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethyl phosphite; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C

2.1: lithium aluminium tetrahydride; aluminum (III) chloride / diethyl ether / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; triethyl phosphite; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ol303518n

Reference yield:

: 1846-69-1
non-2-ynal

: 1421689-41-9
2-(oct-1-yn-1-yl)-1-[2,3,4,5,6-D₅]-phenylazetidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diisopropylamine / hexane; tetrahydrofuran / 0.42 h / -20 - 20 °C / Inert atmosphere

1.2: 0.5 h / -78 - 20 °C / Inert atmosphere

2.1: triethyl phosphite; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C

3.1: lithium aluminium tetrahydride; aluminum (III) chloride / diethyl ether / 0.5 h / 0 - 20 °C / Inert atmosphere

3.2: 0.5 h / Inert atmosphere

With aluminum (III) chloride; lithium aluminium tetrahydride; n-butyllithium; di-isopropyl azodicarboxylate; diisopropylamine; triethyl phosphite; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/ol303518n