Technology Process of C15H17IO5
There total 5 articles about C15H17IO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydrogencarbonate; potassium bromide;
In
dichloromethane;
at -10 - 20 ℃;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium cyanide / water / 30 - 45 °C
2: sulfuric acid / 20 °C
3: 1H-imidazole / dichloromethane; ethyl acetate / 25 - 30 °C
4: N-iodo-succinimide / acetone / 0 - 25 °C
5: sodium hydrogencarbonate; sodium hypochlorite; tetrabutylammomium bromide; dihydrogen peroxide; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / -10 - 20 °C
With
1H-imidazole; sodium cyanide; sodium hypochlorite; N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sulfuric acid; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydrogencarbonate; potassium bromide;
In
dichloromethane; water; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid / 20 °C
2: 1H-imidazole / dichloromethane; ethyl acetate / 25 - 30 °C
3: N-iodo-succinimide / acetone / 0 - 25 °C
4: sodium hydrogencarbonate; sodium hypochlorite; tetrabutylammomium bromide; dihydrogen peroxide; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / -10 - 20 °C
With
1H-imidazole; sodium hypochlorite; N-iodo-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sulfuric acid; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydrogencarbonate; potassium bromide;
In
dichloromethane; ethyl acetate; acetone;