C₃₅H₃₁ClN₂O₅

Base Information

Chemical Name:C₃₅H₃₁ClN₂O₅
CAS No.:1423689-96-6
Molecular Formula:C₃₅H₃₁ClN₂O₅
Molecular Weight:595.095
Hs Code.:

C<sub>35</sub>H<sub>31</sub>ClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₅H₃₁ClN₂O₅

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Chemical Property of C₃₅H₃₁ClN₂O₅

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Technology Process of C₃₅H₃₁ClN₂O₅

There total 15 articles about C₃₅H₃₁ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1423689-93-3
C₄₀H₄₃ClN₂O₅Si

: 1423689-96-6
C₃₅H₃₁ClN₂O₅

Guidance literature:: C₄₀H₄₃ClN₂O₅Si; With hydrogenchloride; In methanol; at 40 ℃; for 4h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1423689-96-6
C₃₅H₃₁ClN₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / dimethyl sulfoxide / 20 °C

2: acetic acid; iron / ethanol / 100 °C

3: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

4: water; sodium hydroxide / methanol; tetrahydrofuran / 20 h / 80 °C

5: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux

6: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 2 h / Reflux; Inert atmosphere

7: hydrogenchloride / methanol / 4 h / 40 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; diphenyl phosphoryl azide; water; iron; sodium hydride; sodium carbonate; potassium carbonate; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423689-96-6
C₃₅H₃₁ClN₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2: diphenyl phosphoryl azide; triethylamine / toluene / 2 h / Reflux

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 2 h / Reflux; Inert atmosphere

4: hydrogenchloride / methanol / 4 h / 40 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; dimethylsulfide borane complex; diphenyl phosphoryl azide; sodium carbonate; triethylamine; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; toluene;