<3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

Base Information

Chemical Name:<3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester
CAS No.:171019-91-3
Molecular Formula:C₃₉H₆₁N₃O₆
Molecular Weight:667.93
Hs Code.:

<3-<N-<4-(carboxyamino)butyl>-16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

Synonyms:<3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

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Chemical Property of <3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

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Technology Process of <3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

There total 6 articles about <3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 171019-90-2
<3--16-<(tetrahydro-2H-pyran-2-yl)oxy>hexadecanamide>propyl>carbamic acid, dibenzyl ester

: 171019-91-3
<3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

Guidance literature:: With acidic Dowex-50 resin; In methanol; for 8h; Ambient temperature;
DOI:10.1016/0040-4020(95)00697-7

Reference yield:

: 124-20-9
N-(3-aminopropyl)-1,4-diaminobutane

: 171019-91-3
<3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / CH₂Cl₂ / 3 h / Ambient temperature

2: 95 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole / tetrahydrofuran / 27 h / Ambient temperature

3: 87 percent / acidic Dowex-50 resin / methanol / 8 h / Ambient temperature

With acidic Dowex-50 resin; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/0040-4020(95)00697-7

Reference yield:

: 74058-68-7
3-benzyloxycarbonyl-1,3-thiazolidine-2-thione

: 171019-91-3
<3--16-hydroxyhexadecanamide>propyl>carbamic acid, dibenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / CH₂Cl₂ / 3 h / Ambient temperature

2: 95 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole / tetrahydrofuran / 27 h / Ambient temperature

3: 87 percent / acidic Dowex-50 resin / methanol / 8 h / Ambient temperature

With acidic Dowex-50 resin; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/0040-4020(95)00697-7