2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene

Base Information

Chemical Name:2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene
CAS No.:637774-33-5
Molecular Formula:C₂₀H₂₂O₆
Molecular Weight:358.391
Hs Code.:

Synonyms:2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene

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Chemical Property of 2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene

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Technology Process of 2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene

There total 1 articles about 2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 118842-88-9
(3-acetyloxy-2-ethoxycarbonylbenzyl)-triphenylphosphonium bromide

: 637774-33-5
2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene

Guidance literature:: With sodium ethanolate; In ethanol; for 24h; Heating;
DOI:10.1016/j.tet.2003.09.046

Reference yield: 96.0%

: 637774-33-5
2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene

: 637774-34-6
2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-carboxy)phenyl)ethene

Guidance literature:: With potassium hydroxide; In ethanol; for 24h; Heating;
DOI:10.1016/j.tet.2003.09.046

Reference yield:

: 637774-33-5
2-(3',4',5'-trimethoxyphenyl)-1-((3-hydroxy-2-ethoxycarbonyl)phenyl)ethene

: 3-(3',4',5'-trimethoxyphenyl)-8-hydroxy-3,4-dihydrobenzopyran-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / KOH / ethanol / 24 h / Heating

2: 55 percent / trifluoroacetic acid / 1,2-dichloro-ethane; H₂O / 28 h / Heating

With potassium hydroxide; trifluoroacetic acid; In ethanol; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2003.09.046