Os3(CO)9(μ3-CO)(μ3-S)

Base Information

Chemical Name:Os3(CO)9(μ3-CO)(μ3-S)
CAS No.:88746-45-6
Molecular Formula:C₁₀O₁₀Os₃S
Molecular Weight:882.77
Hs Code.:

Synonyms:Os3(CO)9(μ3-CO)(μ3-S)

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Chemical Property of Os3(CO)9(μ3-CO)(μ3-S)

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Technology Process of Os3(CO)9(μ3-CO)(μ3-S)

There total 2 articles about Os3(CO)9(μ3-CO)(μ3-S) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 137332-97-9
Os₃(CO)10{SC(H)C₆H₅C(H)C(H)C₆H₅}(H)

: 88746-45-6
Os3(CO)9(μ3-CO)(μ3-S)

: 137333-00-7
H₂Os₆(CO)17(S)(S)

: 137332-98-0
Os₂(CO)7{SC(H)(C₆H₄)CH₂CH₂C₆H₅}

Guidance literature:: With CO; In octane; heating of the Os3 cluster in octane under an atmosphere of CO (125°C, 2 h), color change from yellow to red;
DOI:10.1021/om00037a024

Reference yield: 24.0%

: {Os3(CO)10(μH)(μSC6H5)}

: 88746-45-6
Os3(CO)9(μ3-CO)(μ3-S)

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

Guidance literature:: In further solvent(s); Irradiation (UV/VIS); a soln. of HOs3(CO)10(SPh) in nonane was photolyzed (external high pressure Hg lamp, Pyrex glassware) in a sealed tube under CO (1 atm) for 4 h; solvent was removed in vacuo, residue chromd. on silica TLC plates (eluent benzene-CH2Cl2); yield of benzene was detd. by GC of the reaction mixt.;

Reference yield: 27.0%

: 42565-94-6
dimethylphenylphosphine(carbonyl)5tungsten

: 88746-45-6
Os3(CO)9(μ3-CO)(μ3-S)

: 119454-95-4
Os3W(CO)11(P(CH3)2C6H5)2(μ3-S)

Guidance literature:: In hexane; Irradiation (UV/VIS); a hexane soln. of Os3(CO)9(μ3-CO)(μ3-S) and W(CO)5(PMe2Ph) was irradiated (UV) for 1 h under a slow purge with N2; isolated by TLC;