C₃₁H₅₀OSi

Base Information

Chemical Name:C₃₁H₅₀OSi
CAS No.:934808-38-5
Molecular Formula:C₃₁H₅₀OSi
Molecular Weight:466.823
Hs Code.:

Synonyms:C₃₁H₅₀OSi

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Chemical Property of C₃₁H₅₀OSi

Chemical Property:

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Technology Process of C₃₁H₅₀OSi

There total 2 articles about C₃₁H₅₀OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934558-86-8
C₂₆H₄₀O₂Si

: 934808-38-5
C₃₁H₅₀OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: NMO; TPAP; 4 Angstroem MS / CH₂Cl₂ / 0.5 h / 25 °C

1.2: 65 percent / toluene / 12 h / 80 °C

2.1: H₂ / irridium catalyst / CH₂Cl₂ / 4 h / 25 °C / 38002.6 Torr

2.2: 80 percent / DIBALH / tetrahydrofuran; CH₂Cl₂ / 0.5 h / 0 °C

3.1: NMO; TPAP; 4 Angstroem MS / CH₂Cl₂ / 0.5 h / 25 °C

3.2: tetrahydrofuran; toluene / 1 h / -78 °C

3.3: 76 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 7 h / 25 °C

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroem MS; hydrogen; irridium catalyst; In dichloromethane;
DOI:10.1021/ol070298z

Reference yield:

: 934808-36-3
C₃₀H₄₄O₃Si

: 934808-38-5
C₃₁H₅₀OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / irridium catalyst / CH₂Cl₂ / 4 h / 25 °C / 38002.6 Torr

1.2: 80 percent / DIBALH / tetrahydrofuran; CH₂Cl₂ / 0.5 h / 0 °C

2.1: NMO; TPAP; 4 Angstroem MS / CH₂Cl₂ / 0.5 h / 25 °C

2.2: tetrahydrofuran; toluene / 1 h / -78 °C

2.3: 76 percent / H₂ / Pd/C / tetrahydrofuran; methanol / 7 h / 25 °C

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 Angstroem MS; hydrogen; irridium catalyst; In dichloromethane;
DOI:10.1021/ol070298z