Technology Process of C28H29NO2
There total 4 articles about C28H29NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; caesium carbonate; XPhos;
In
toluene;
at 180 ℃;
for 10h;
Sealed tube;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere
1.2: 5 h / 25 °C
2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 25 °C
3.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C
4.1: caesium carbonate; palladium diacetate; XPhos / toluene / 10 h / 180 °C / Sealed tube; Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; palladium diacetate; sodium hydride; caesium carbonate; triethylamine; XPhos;
In
tetrahydrofuran; dichloromethane; ethyl acetate; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 5 h / 0 - 20 °C
2: caesium carbonate; palladium diacetate; XPhos / toluene / 10 h / 180 °C / Sealed tube; Inert atmosphere
With
palladium diacetate; caesium carbonate; triethylamine; XPhos;
In
dichloromethane; toluene;