Technology Process of C54H48FN5O7
There total 22 articles about C54H48FN5O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 20 °C / Cooling with ice
2: dmap / dichloromethane / 0 - 20 °C
3: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C
4: ammonia / methanol / 18 h / 20 °C
5: 1H-imidazole; pyridine / 15 h / 0 - 20 °C
6: silver nitrate / dichloromethane / 20 °C / Inert atmosphere
7: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C
With
pyridine; 1H-imidazole; dmap; N-iodo-succinimide; 15-crown-5; tetrabutyl ammonium fluoride; ammonia; silver nitrate; triethylamine tris(hydrogen fluoride);
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap / dichloromethane / 0 - 20 °C
2: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C
3: ammonia / methanol / 18 h / 20 °C
4: 1H-imidazole; pyridine / 15 h / 0 - 20 °C
5: silver nitrate / dichloromethane / 20 °C / Inert atmosphere
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C
With
pyridine; 1H-imidazole; dmap; 15-crown-5; tetrabutyl ammonium fluoride; ammonia; silver nitrate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C
2: ammonia / methanol / 18 h / 20 °C
3: 1H-imidazole; pyridine / 15 h / 0 - 20 °C
4: silver nitrate / dichloromethane / 20 °C / Inert atmosphere
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C
With
pyridine; 1H-imidazole; 15-crown-5; tetrabutyl ammonium fluoride; ammonia; silver nitrate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;