Technology Process of C45H56N6O11
There total 7 articles about C45H56N6O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
dimethyl sulfoxide;
at 80 ℃;
for 72h;
Inert atmosphere;
DOI:10.1021/ja412729s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / 1,4-dioxane; water / 16 h / 20 °C / Inert atmosphere
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
3: dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere
4: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 72 h / 80 °C / Inert atmosphere
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide;
In
1,4-dioxane; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja412729s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
2: dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 72 h / 80 °C / Inert atmosphere
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja412729s