5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole

Base Information

Chemical Name:5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole
CAS No.:1309760-70-0
Molecular Formula:C₂₆H₂₄N₄O₂
Molecular Weight:424.502
Hs Code.:

Synonyms:5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole

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Chemical Property of 5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole

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Technology Process of 5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole

There total 3 articles about 5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1309760-67-5
5,6-dimethyl-9-methoxy-1-(4'-aminophenyl)-6H-pyrido[4,3-b]carbazole

: 624-83-9
methyl isocyanate

: 1309760-70-0
5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole

Guidance literature:: 5,6-dimethyl-9-methoxy-1-(4'-aminophenyl)-6H-pyrido[4,3-b]carbazole; With dmap; In chloroform; for 0.5h;

methyl isocyanate; In chloroform; at 20 ℃; for 24h;

Reference yield:

: 889653-92-3
9-methoxy-5-methyl-1-(4-nitro-phenyl)-6H-pyrido[4,3-b]carbazole

: 1309760-70-0
5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: 18-crown-6 ether; potassium carbonate

2.1: palladium 10% on activated carbon; hydrogen; acetic acid / 50 °C

3.1: dmap / chloroform / 0.5 h

3.2: 24 h / 20 °C

With dmap; 18-crown-6 ether; palladium 10% on activated carbon; hydrogen; potassium carbonate; acetic acid; In chloroform;

Reference yield:

: 889653-94-5
5,6-dimethyl-9-methoxy-1-(4'-nitrophenyl)-6H-pyrido[4,3-b]carbazole

: 1309760-70-0
5,6-dimethyl-9-methoxy-1-[4'-(3-methylureilene)phenyl]-6H-pyrido[4,3-b]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon; hydrogen; acetic acid / 50 °C

2.1: dmap / chloroform / 0.5 h

2.2: 24 h / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; acetic acid; In chloroform;