2,2'-((Methylenedioxy)di-p-phenylene)disuccinimide

Base Information

Chemical Name:2,2'-((Methylenedioxy)di-p-phenylene)disuccinimide
CAS No.:87367-86-0
Molecular Formula:C₂₁H₁₈N₂O₆
Molecular Weight:394.384
Hs Code.:
DSSTox Substance ID:DTXSID601007506

Synonyms:87367-86-0;BRN 5651241;2,2'-((Methylenedioxy)di-p-phenylene)disuccinimide;Succinimide, 2,2'-((methylenedioxy)di-p-phenylene)di-;3,3'-((Methylenebis(oxy))bis(4,1-phenylene))bis(pyrrolidine-2,5-dione);Oprea1_215261;DTXSID601007506;LS-147615;3,3'-[Methylenebis(oxy-4,1-phenylene)]bis(5-hydroxy-3,4-dihydro-2H-pyrrol-2-one)

Suppliers and Price of 2,2'-((Methylenedioxy)di-p-phenylene)disuccinimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-((Methylenedioxy)di-p-phenylene)disuccinimide

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:394.11648630
Heavy Atom Count:29
Complexity:608

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(C(=O)NC1=O)C2=CC=C(C=C2)OCOC3=CC=C(C=C3)C4CC(=O)NC4=O

Technology Process of 2,2'-((Methylenedioxy)di-p-phenylene)disuccinimide

There total 4 articles about 2,2'-((Methylenedioxy)di-p-phenylene)disuccinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77354-99-5
4,4'-[methylenebis(oxy)]bis benzaldehyde

: 87367-86-0
4,4'-(Methylenedioxy)diphenylsuccinimide

Guidance literature:: Multi-step reaction with 4 steps

1: 80.5 percent / piperidine, glacial acetic acid / benzene / Heating

2: 2.) NaOH / 1.) water, ethanol, heating, 2 h, 2.) ethylene glycol, heating, 40 h

3: 1.) acetic anhydride, 2.) ammonia / 1.) heating, 6 h, 2.) ethyl acetate, 2 h

4: 1 h / 200 - 220 °C

With piperidine; sodium hydroxide; ammonia; acetic anhydride; acetic acid; In benzene;
DOI:10.1007/BF00765771

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 87367-86-0
4,4'-(Methylenedioxy)diphenylsuccinimide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaOEt / 1.) ethanol, reflux, 4 h, 2.) reflux, 48 h

2: 80.5 percent / piperidine, glacial acetic acid / benzene / Heating

3: 2.) NaOH / 1.) water, ethanol, heating, 2 h, 2.) ethylene glycol, heating, 40 h

4: 1.) acetic anhydride, 2.) ammonia / 1.) heating, 6 h, 2.) ethyl acetate, 2 h

5: 1 h / 200 - 220 °C

With piperidine; sodium hydroxide; ammonia; sodium ethanolate; acetic anhydride; acetic acid; In benzene;
DOI:10.1007/BF00765771