(2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine

Base Information

Chemical Name:(2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine
CAS No.:137934-47-5
Molecular Formula:C₂₈H₂₈INO₂S
Molecular Weight:569.506
Hs Code.:

Synonyms:(2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine

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Technology Process of (2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine

There total 2 articles about (2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 262846-22-0
(2S,4S)-2-(Toluene-4-sulfonyloxymethyl)-4-tritylsulfanyl-pyrrolidine-1-carboxylic acid allyl ester

: 137934-47-5
(2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine

Guidance literature:: With sodium iodide; In acetone; at 50 ℃;
DOI:10.1016/S0960-894X(99)00657-5

Reference yield:

: 133995-30-9
(2S,4S)-2-hydroxymethyl-4-tritylthio-1-(allyloxycarbonyl)pyrrolidine

: 137934-47-5
(2S,4S)-N-allyloxycarbonyl-2-iodomethyl-4-triphenylmethylthiopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / TEA / dimethylformamide / 20 °C

2: 78 percent / NaI / acetone / 50 °C

With TEA; sodium iodide; In N,N-dimethyl-formamide; acetone; 1: Tosylation / 2: Iodination;
DOI:10.1016/S0960-894X(99)00657-5